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Maestría
Secado por aspersión de mucílago de nopal (Opuntia ficus indica) y su efecto en las propiedades reológicas de los polvos reconstituidos
Titre : Secado por aspersión de mucílago de nopal (Opuntia ficus indica) y su efecto en las propiedades reológicas de los polvos reconstituidos
Auteur : León Martínez, Frank Manuel
Etablissement de soutenance : Instituto Politécnico Nacional (IPN)
Grade : Maestria en Ciencias 2010
Résumé
Currently
,
there is
a
marked
interest
by
the use of the specie
Opuntia ficus indica
, due to
its ability to develop in adverse environments.
Fruits, stems and extracts are used to multiple
uses. In particular
case,
the mucilage
generated by this species has been studied by its
physicochemical properties
and rheological
properties
. However
, the
shelf
life of the extract
is very limited, given its high water activity (>0.8) and chemical composition
(polysaccharides).
The bio-polymer stabilization has not been studied thoroughly, and is of vital importance
an analysis of processing alternatives if it industrial level is wished.
In this study was evaluated the use of the spray drying in aqueous extracts of
O. ficus
indica
mucilage
without the
addition of a drying agent
at pilot scale.
These
studies may help
in the determination of factors that affecting the drying process, as well in the
process
optimization in function of
material response, without the needs
to invert much economic
resources
.
A
2
3
factorial design with three central points w
as used for analyze the effects of
the spray-drying conditions on the dehydrated mucilage properties.
The effects of
inlet air
temperature, feed flow rate, and atomizer speed on the rheological properties (elastic and
viscous), as well the particle size distribution of mucilage reconstituted solutions at different
concentrations were evaluated.
In addition,
the effects of the drying conditions on powder
properties bulk density, moisture content, and yield were considered.
It was elected a sample
of mucilage
powder to determine glass transition temperature (T
g
), water adsorption
behavior, and particle morphology.
The results indicated that mucilage powders obtained had low higroscopicity for a
w
<
0.6
and with values of T
g
higher than the
room temperature.
In general, the mucilage
reconstituted
solutions exhibited a non-Newtonian
“shear thinning”
behavior, with important
viscoelastic properties at high
concentrations,
composed of particles in agglomerated
structure.
The best spray drying conditions founded
for the production of mucilage powder
with low moisture content
,
high bulk density
, and
acceptable
rheological properties
were
with inlet temperature of 130
°C, a feed flow rate of 2.3 L/h, and speed atomizer of 2
1000
rpm
.
Page publiée le 11 juin 2015, mise à jour le 20 août 2017